In-situ Al 2O 3 (14.8–31.3 wt.%) reinforced Fe–Cr–Ni alloys were prepared using reactive hot pressing at a temperature of 700°C and pressure of 30 MPa for 2 h. X-ray diffraction showed that the obtained metal matrix composites (MMCs) mainly comprised Al 2O 3, Fe–Cr and Cr 0.7Fe 0.36Ni 2.9 phases. Vickers hardness values of the composites with varying Al 2O 3 contents were all around 4.28 GPa. Scanning electron microscopy images showed that the Al 2O 3 particles in the MMCs (with Al 2O 3 content of 14.8 wt.%) were ultrafine and uniformly distributed. Moreover, the metal matrix composite with 14.8 wt.% Al 2O 3 exhibited the highest values of fracture toughness and bending strength, which were 15.2 MPa · m 1/2 and 529 MPa, respectively.