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      Microwave Assisted Extraction of Phenolic Compounds from Four Different Spices

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          Abstract

          Spices and herbs are known not only for their taste, aroma and flavour, but also for their medical properties and value. Both spices and herbs have been used for centuries in traditional medical systems to cure various kinds of illnesses such as common cold, diabetes, cough and cancers. The aim of this work was the comparison between two different extractive techniques in order to get qualitative and quantitative data regarding bioactive compounds of four different spices ( Cinnamomum zeylanicum, Coriandrum sativum, Cuminum cyminum, Crocus sativus). The plants were extracted employing ultrasonication and microwave-assisted extractions. The efficiency of extraction of bioactive compounds obtained with the microwave extraction process was in general about four times higher than that resulting from sonication extraction. The various extracts obtained were analyzed for their antioxidant activity using ABTS, DPPH and FRAP assays and for their total polyphenolic content. It can be concluded that microwave-assisted extractions provide significant advantages in terms of extraction efficiency and time savings.

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          Most cited references34

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          Antioxidant Activity of Various Tea Extracts in Relation to Their Antimutagenicity

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            Antioxidant capacity of 26 spice extracts and characterization of their phenolic constituents.

            Total equivalent antioxidant capacity (TEAC) and phenolic content of 26 common spice extracts from 12 botanical families were investigated. Qualitative and quantitative analyses of major phenolics in the spice extracts were systematically conducted by reversed-phase high-performance liquid chromatography (RP-HPLC). Many spices contained high levels of phenolics and demonstrated high antioxidant capacity. Wide variation in TEAC values (0.55-168.7 mmol/100 g) and total phenolic content (0.04-14.38 g of gallic acid equivalent/100 g) was observed. A highly positive linear relationship (R2= 0.95) obtained between TEAC values and total phenolic content showed that phenolic compounds in the tested spices contributed significantly to their antioxidant capacity. Major types of phenolic constituents identified in the spice extracts were phenolic acids, phenolic diterpenes, flavonoids, and volatile oils (e.g., aromatic compounds). Rosmarinic acid was the dominant phenolic compound in the six spices of the family Labiatae. Phenolic volatile oils were the principal active ingredients in most spices. The spices and related families with the highest antioxidant capacity were screened, e.g., clove in the Myrtaceae, cinnamon in the Lauraceae, oregano in the Labiatae, etc., representing potential sources of potent natural antioxidants for commercial exploitation. This study provides direct comparative data on antioxidant capacity and total and individual phenolics contents of the 26 spice extracts.
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              The Relative Antioxidant Activities of Plant-Derived Polyphenolic Flavonoids

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                Author and article information

                Journal
                Molecules
                Molecules
                molecules
                Molecules
                MDPI
                1420-3049
                09 September 2010
                September 2010
                : 15
                : 9
                : 6365-6374
                Affiliations
                Department of Food Science, University of Naples “Federico II”, Via Università 100, Parco Gussone Ed.84, 80055, Portici, Naples, Italy
                Author notes
                [* ]Author to whom correspondence should be addressed; E-Mail: giulia.graziani@ 123456unina.it ; Tel.: +39812539351; Fax: +39817762580.
                Article
                molecules-15-06365
                10.3390/molecules15096365
                6257672
                20877228
                096cd04a-a862-48ba-be05-ce5bf614a0a3
                © 2010 by the authors;

                licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution license ( http://creativecommons.org/licenses/by/3.0/).

                History
                : 09 July 2010
                : 28 July 2010
                : 30 July 2010
                Categories
                Article

                spices,antioxidant activity,phenolic compounds,mae,food composition

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