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      Direct evidence on the existence of [Mo132]Keplerate-type species in aqueous solution.

      Inorganic Chemistry

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          Abstract

          We demonstrate the existence of discrete single molecular [Mo(132)] Keplerate-type clusters in aqueous solution. Starting from a discrete spherical [Mo(132)] cluster, the formation of an open-basket-type [Mo(116)] defect structure is shown for the first time in solution using analytical ultracentrifugation sedimentation velocity experiments.

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          Journal
          17850076
          10.1021/ic701076s

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