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      Small-angle X-ray scattering (SAXS) off parallel, cylindrical, well-defined nanopores: from random pore distribution to highly ordered samples

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          Freestanding, Highly Flexible, Large Area, Nanoporous Alumina Membranes with Complete Through-Hole Pore Morphology

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            Capillary Filling of Anodized Alumina Nanopore Arrays

            The filling behavior of a room temperature solvent, perfluoromethylcyclohexane, in approximately 20 nm nanoporous alumina membranes was investigated in situ with small angle x-ray scattering. Adsorption in the pores was controlled reversibly by varying the chemical potential between the sample and a liquid reservoir via a thermal offset, \(\Delta\)T. The system exhibited a pronounced hysteretic capillary filling transition as liquid was condensed into the nanopores. These results are compared with Kelvin-Cohan theory, with a modified Derjaguin approximation, as well as with predictions by Cole and Saam.
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              Author and article information

              Journal
              Applied Physics A
              Appl. Phys. A
              Springer Nature
              0947-8396
              1432-0630
              October 2009
              July 2009
              : 97
              : 1
              : 99-108
              Article
              10.1007/s00339-009-5346-4
              60c9b472-6f32-4ea2-9b02-ca052c46b319
              © 2009
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              Self URI (article page): http://link.springer.com/10.1007/s00339-009-5346-4

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