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      Compressive properties of self-healing microcapsule-based cementitious composites subjected to freeze-thaw cycles using acoustic emission

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          Abstract

          Microcapsule self-healing technology is an effective scheme to improve the durability of cementitious composites. In this paper, the compressive properties of microcapsule-based self-healing cementitious composites after freeze-thaw cycles were studied using acoustic emission (AE), and the changes in AE characteristics, compressive strength, mass loss rate, and electric flux of microcapsule-based self-healing cementitious composites with different microcapsule contents and freeze-thaw cycles were studied. The results show that if the content of the microcapsule is appropriate, with the increase in the number of freeze-thaw cycles, the AE hits will generally increase first and then decrease, and the early AE events will also decrease. Because of the different contents of microcapsules, the improvement effect and defect effect change dynamically with the number of freeze-thaw cycles, which is also reflected in the dynamic process of compressive strength. After 100 freeze-thaw cycles, the compressive strength of self-healing cementitious composite samples with 5% content of microcapsules and 3% content of microcapsules is the highest. The changes in mass loss rate and electric flux are similar to the AE characteristic parameters, which further verifies the results of AE. The research results of this paper provide experimental data and experimental methods for the engineering application of microcapsule self-healing cement-based composites in cold areas.

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          Most cited references23

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          Autonomic healing of polymer composites.

          Structural polymers are susceptible to damage in the form of cracks, which form deep within the structure where detection is difficult and repair is almost impossible. Cracking leads to mechanical degradation of fibre-reinforced polymer composites; in microelectronic polymeric components it can also lead to electrical failure. Microcracking induced by thermal and mechanical fatigue is also a long-standing problem in polymer adhesives. Regardless of the application, once cracks have formed within polymeric materials, the integrity of the structure is significantly compromised. Experiments exploring the concept of self-repair have been previously reported, but the only successful crack-healing methods that have been reported so far require some form of manual intervention. Here we report a structural polymeric material with the ability to autonomically heal cracks. The material incorporates a microencapsulated healing agent that is released upon crack intrusion. Polymerization of the healing agent is then triggered by contact with an embedded catalyst, bonding the crack faces. Our fracture experiments yield as much as 75% recovery in toughness, and we expect that our approach will be applicable to other brittle materials systems (including ceramics and glasses).
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            Self-healing concrete composites for sustainable infrastructures: A review

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              On acoustic emission characteristics, initiation crack intensity, and damage evolution of cement-paste backfill under uniaxial compression

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                Author and article information

                Contributors
                Journal
                Front Chem
                Front Chem
                Front. Chem.
                Frontiers in Chemistry
                Frontiers Media S.A.
                2296-2646
                23 September 2022
                2022
                : 10
                : 940184
                Affiliations
                [ 1 ] College of Mechanical Engineering , Yangzhou University , Yangzhou, China
                [ 2 ] Faculty of Civil Engineering and Mechanics , Jiangsu University , Zhenjiang, China
                Author notes
                *Correspondence: Wenfeng Hao, hwf@ 123456yzu.edu.cn ; Shiping Jiang, spjiangvip@ 123456126.com

                This article was submitted to Polymer Chemistry, a section of the journal Frontiers in Chemistry

                Edited by: Narsimha Mamidi, Monterrey Institute of Technology and Higher Education (ITESM), Mexico

                Reviewed by: Widya Fatriasari, Widya Fatriasari, Indonesia

                Adreeja Basu, Indian Institute of Technology Guwahati, India

                Manoj Kumar Karnena, Gandhi Institute of Technology and Management (GITAM), India

                Madhavi Konni, Malla Reddy Engineering College, India

                Article
                940184
                10.3389/fchem.2022.940184
                9537771
                6762dcd9-b00c-45e7-9479-76a2b6d8a056
                Copyright © 2022 Hao, Hao, Kanwal and Jiang.

                This is an open-access article distributed under the terms of the Creative Commons Attribution License (CC BY). The use, distribution or reproduction in other forums is permitted, provided the original author(s) and the copyright owner(s) are credited and that the original publication in this journal is cited, in accordance with accepted academic practice. No use, distribution or reproduction is permitted which does not comply with these terms.

                History
                : 10 May 2022
                : 29 August 2022
                Categories
                Chemistry
                Original Research

                self-healing cementitious composites,freeze-thaw cycles,acoustic emission,compressive properties,microcapsules,frost resistance

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