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      Microstructure and properties of hot extruded Mg-3Zn-Y- xCu ( x = 0, 1, 3, 5) alloys

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          Abstract

          In petroleum drilling engineering, materials with high strength and rapid degradation are required for degradable fracturing ball applications. In this work, the microstructure, mechanical properties, and corrosion behavior of extruded Mg-3Zn-Y- xCu ( x = 0, 1, 3, 5 weight percent) alloys are investigated using optical microscopy, scanning electronic microscopy equipped with energy dispersive X-ray spectroscopy, X-ray diffraction, transmission electronic microscopy, compression tests, electrochemical measurements, and hydrogen evolution tests, to explore their potential as excellent candidate alloys for degradable fracturing ball applications. It is found that the Mg-3Zn-Y alloy is mainly composed of α-Mg, Mg 3Zn 3Y 2, and Mg 3Zn 6Y phases. After Cu addition, a new MgZnCu phase is formed, while the Mg 3Zn 3Y 2 phase disappears. The Mg-3Zn-Y-3Cu alloy shows the highest compressive strength (473 MPa) and yield strength (402 MPa), mainly attributed to the combined effect of the fine-grain and dispersed precipitation of Mg 3Zn 6Y and MgZnCu. The corrosion rate of Mg-3Zn-Y-3Cu reaches 0.41 mm day −1 in 3.5 wt.% KCl solution. Consequently, Mg-3Zn-Y-3Cu alloy is a suitable degradable fracturing ball-seat material.

          Author and article information

          Journal
          ijmr
          International Journal of Materials Research
          Carl Hanser Verlag
          1862-5282
          2195-8556
          13 April 2017
          : 108
          : 4
          : 262-268
          Affiliations
          a College of Materials Science and Engineering, Taiyuan University of Science and Technology, Taiyuan, P. R. China
          b Engineering Research Center for Magnesium Alloys of Shanxi Province, Taiyuan University of Science and Technology, Taiyuan, P. R. China
          c College of Chemical and Biological Engineering, Taiyuan University of Science and Technology, Taiyuan, P. R. China
          Author notes
          [* ] Correspondence address, Professor Da-qing Fang, School of Materials Science and Engineering, Taiyuan University of Science and Technology, Taiyuan, 030024, P. R. China, Tel.: +86-351-6998145, Fax: +86-351-6998145, E-mail: fangdaqingtykd@ 123456163.com
          Article
          MK111476
          10.3139/146.111476
          734c983d-2f31-42c9-a43c-f2c2a83e2e5d
          © 2017, Carl Hanser Verlag, München
          History
          : 6 December 2016
          : 10 January 2017
          : 2 February 2017
          Page count
          References: 33, Pages: 7
          Categories
          Original Contributions

          Materials technology,Materials characterization,Materials science
          Microstructure,Hot extruded,Mechanical properties,Corrosion behavior,Degradable magnesium alloys

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