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      Precise wavefront characterization of x-ray optical elements using a laboratory source

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          Abstract

          Improvements in x-ray optics critically depend on the measurement of their optical performance. The knowledge of wavefront aberrations, for example, can be used to improve the fabrication of optical elements or to design phase correctors to compensate for these errors. At present, the characterization of such optics is made using intense x-ray sources, such as synchrotrons. However, the limited access to these facilities can substantially slow down the development process. Improvements in the brightness of lab-based x-ray micro-sources in combination with the development of new metrology methods, particularly ptychographic x-ray speckle tracking, enable characterization of x-ray optics in the lab with a precision and sensitivity not possible before. Here, we present a laboratory setup that utilizes a commercially available x-ray source and can be used to characterize different types of x-ray optics. The setup is used in our laboratory on a routine basis to characterize multilayer Laue lenses of high numerical aperture and other optical elements. This typically includes measurements of the wavefront distortions, optimum operating photon energy, and focal length of the lens. To check the sensitivity and accuracy of this laboratory setup, we compared the results to those obtained at the synchrotron and saw no significant difference. To illustrate the feedback of measurements on performance, we demonstrated the correction of the phase errors of a particular multilayer Laue lens using a 3D printed compound refractive phase plate.

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          X-Ray Interactions: Photoabsorption, Scattering, Transmission, and Reflection at E = 50-30,000 eV, Z = 1-92

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            X-ray phase imaging with a paper analyzer

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              Speckle-based x-ray phase-contrast and dark-field imaging with a laboratory source.

              We report on the observation and application of near-field speckles with a laboratory x-ray source. The detection of speckles is possible thanks to the enhanced brilliance properties of the used liquid-metal-jet source, and opens the way to a range of new applications in laboratory-based coherent x-ray imaging. Here, we use the speckle pattern for multimodal imaging of demonstrator objects. Moreover, we introduce algorithms for phase and dark-field imaging using speckle tracking, and we show that they yield superior results with respect to existing methods.
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                Author and article information

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                Journal
                Review of Scientific Instruments
                Review of Scientific Instruments
                AIP Publishing
                0034-6748
                1089-7623
                July 01 2022
                July 01 2022
                : 93
                : 7
                : 073704
                Affiliations
                [1 ]The Hamburg Centre for Ultrafast Imaging, Luruper Chaussee 149, 22761 Hamburg, Germany
                [2 ]Center for Free-Electron Laser Science CFEL, Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
                [3 ]School of Physics, University of Melbourne, Parkville, Victoria 3010, Australia
                [4 ]Department of Physics, Universität Hamburg, Luruper Chaussee 149, 22761 Hamburg, Germany
                Article
                10.1063/5.0092269
                35922318
                842d52f2-3dcf-4015-b639-5823982edf7d
                © 2022
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