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      Discrete shear band plasticity through dislocation activities in body-centered cubic tungsten nanowires

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          Abstract

          Shear band in metallic crystals is localized deformation with high dislocation density, which is often observed in nanopillar deformation experiments. The shear band dynamics coupled with dislocation activities, however, remains unclear. Here, we investigate the dynamic processes of dislocation and shear band in body-centered cubic (BCC) tungsten nanowires via an integrated approach of in situ nanomechanical testing and atomistic simulation. We find a strong effect of surface orientation on dislocation nucleation in tungsten nanowires, in which {111} surfaces act as favorite sites under high strain. While dislocation activities in a localized region give rise to an initially thin shear band, self-catalyzed stress concentration and dislocation nucleation at shear band interfaces cause a discrete thickening of shear band. Our findings not only advance the current understanding of defect activities and deformation morphology of BCC nanowires, but also shed light on the deformation dynamics in other microscopic crystals where jerky motion of deformation band is observed.

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          Most cited references28

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          Sample dimensions influence strength and crystal plasticity.

          When a crystal deforms plastically, phenomena such as dislocation storage, multiplication, motion, pinning, and nucleation occur over the submicron-to-nanometer scale. Here we report measurements of plastic yielding for single crystals of micrometer-sized dimensions for three different types of metals. We find that within the tests, the overall sample dimensions artificially limit the length scales available for plastic processes. The results show dramatic size effects at surprisingly large sample dimensions. These results emphasize that at the micrometer scale, one must define both the external geometry and internal structure to characterize the strength of a material.
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            Size dependence of mechanical properties of gold at the micron scale in the absence of strain gradients

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              Mechanical annealing and source-limited deformation in submicrometre-diameter Ni crystals.

              The fundamental processes that govern plasticity and determine strength in crystalline materials at small length scales have been studied for over fifty years. Recent studies of single-crystal metallic pillars with diameters of a few tens of micrometres or less have clearly demonstrated that the strengths of these pillars increase as their diameters decrease, leading to attempts to augment existing ideas about pronounced size effects with new models and simulations. Through in situ nanocompression experiments inside a transmission electron microscope we can directly observe the deformation of these pillar structures and correlate the measured stress values with discrete plastic events. Our experiments show that submicrometre nickel crystals microfabricated into pillar structures contain a high density of initial defects after processing but can be made dislocation free by applying purely mechanical stress. This phenomenon, termed 'mechanical annealing', leads to clear evidence of source-limited deformation where atypical hardening occurs through the progressive activation and exhaustion of dislocation sources.
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                Author and article information

                Contributors
                jiangwei_wang@zju.edu.cn
                caiwei@stanford.edu
                sxm2@pitt.edu
                Journal
                Sci Rep
                Sci Rep
                Scientific Reports
                Nature Publishing Group UK (London )
                2045-2322
                15 March 2018
                15 March 2018
                2018
                : 8
                : 4574
                Affiliations
                [1 ]ISNI 0000 0004 1759 700X, GRID grid.13402.34, Center of Electron Microscopy and State Key Laboratory of Silicon Materials, School of Materials Science and Engineering, , Zhejiang University, ; Hangzhou, 310027 China
                [2 ]ISNI 0000 0004 1936 9000, GRID grid.21925.3d, Department of Mechanical Engineering and Materials Science, , University of Pittsburgh, ; Pittsburgh, Pennsylvania 15261 USA
                [3 ]ISNI 0000 0001 2341 2786, GRID grid.116068.8, Research Laboratory of Electronics, , Massachusetts Institute of Technology, ; Cambridge, Massachusetts 02139 USA
                [4 ]ISNI 0000000419368956, GRID grid.168010.e, Department of Mechanical Engineering, , Stanford University, ; Stanford, California 94305 USA
                Article
                23015
                10.1038/s41598-018-23015-z
                5854623
                29545583
                9b39cba4-ee52-4154-b16c-b00b89e35155
                © The Author(s) 2018

                Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made. The images or other third party material in this article are included in the article’s Creative Commons license, unless indicated otherwise in a credit line to the material. If material is not included in the article’s Creative Commons license and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this license, visit http://creativecommons.org/licenses/by/4.0/.

                History
                : 6 December 2017
                : 5 March 2018
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