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      Three-dimensional diffraction mapping by tuning the X-ray energy

      a , * , a , a , a , a , b

      Journal of Synchrotron Radiation

      International Union of Crystallography

      Includes papers presented at the Sixth International Workshop on X-ray Radiation Damage to Biological Crystalline Samples

      X-ray diffraction, nanofocused and microfocused XRD, energy scan, three-dimensional reciprocal-space mapping

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          Abstract

          Three-dimensional reciprocal-space maps of a single SiGe island around the Si(004) Bragg peak are recorded using an energy-tuning technique with a microfocused X-ray beam with compound refractive lenses as focusing optics.

          Abstract

          Three-dimensional reciprocal-space maps of a single SiGe island around the Si(004) Bragg peak are recorded using an energy-tuning technique with a microfocused X-ray beam with compound refractive lenses as focusing optics. The map is in agreement with simulated data as well as with a map recorded by an ordinary rocking-curve scan. The energy-tuning approach circumvents both the comparatively large sphere of confusion of diffractometers compared with nanostructures and vibrations induced by motors. Thus, this method offers new possibilities for novel combinations of three-dimensional micro- and nano-focused X-ray diffraction with complex in situ sample environments such as scanning probe microscopes.

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          Author and article information

          Affiliations
          [a ]simpleEuropean Synchrotron Radiation Facility , 6 rue Jules Horowitz, BP 220, 38043 Grenoble Cedex, France
          [b ]simpleMax Planck Institute of Colloids and Interfaces , 14424 Potsdam, Germany
          Author notes
          Correspondence e-mail: thomas.cornelius@ 123456esrf.fr
          Conference
          J Synchrotron Radiat
          J. Synchrotron Rad.
          Journal of Synchrotron Radiation
          International Union of Crystallography
          0909-0495
          1600-5775
          01 May 2011
          15 March 2011
          15 March 2011
          : 18
          : Pt 3 ( publisher-idID: s110300 )
          : 413-417
          3268694
          21525649
          vv5013
          10.1107/S0909049511003190
          JSYRES S0909049511003190
          © T. W. Cornelius et al. 2011

          This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.

          Includes papers presented at the Sixth International Workshop on X-ray Radiation Damage to Biological Crystalline Samples
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          Research Papers

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