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Three-dimensional diffraction mapping by tuning the X-ray energy

a , * , a , a , a , a , b

Journal of Synchrotron Radiation

International Union of Crystallography

Includes papers presented at the Sixth International Workshop on X-ray Radiation Damage to Biological Crystalline Samples

X-ray diffraction, nanofocused and microfocused XRD, energy scan, three-dimensional reciprocal-space mapping

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      Abstract

      Three-dimensional reciprocal-space maps of a single SiGe island around the Si(004) Bragg peak are recorded using an energy-tuning technique with a microfocused X-ray beam with compound refractive lenses as focusing optics.

      Abstract

      Three-dimensional reciprocal-space maps of a single SiGe island around the Si(004) Bragg peak are recorded using an energy-tuning technique with a microfocused X-ray beam with compound refractive lenses as focusing optics. The map is in agreement with simulated data as well as with a map recorded by an ordinary rocking-curve scan. The energy-tuning approach circumvents both the comparatively large sphere of confusion of diffractometers compared with nanostructures and vibrations induced by motors. Thus, this method offers new possibilities for novel combinations of three-dimensional micro- and nano-focused X-ray diffraction with complex in situ sample environments such as scanning probe microscopes.

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      Affiliations
      [a ]simpleEuropean Synchrotron Radiation Facility , 6 rue Jules Horowitz, BP 220, 38043 Grenoble Cedex, France
      [b ]simpleMax Planck Institute of Colloids and Interfaces , 14424 Potsdam, Germany
      Author notes
      Correspondence e-mail: thomas.cornelius@ 123456esrf.fr
      Conference
      J Synchrotron Radiat
      J. Synchrotron Rad.
      Journal of Synchrotron Radiation
      International Union of Crystallography
      0909-0495
      1600-5775
      01 May 2011
      15 March 2011
      15 March 2011
      : 18
      : Pt 3 ( publisher-idID: s110300 )
      : 413-417
      3268694
      21525649
      vv5013
      10.1107/S0909049511003190
      JSYRES S0909049511003190
      © T. W. Cornelius et al. 2011

      This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.

      Includes papers presented at the Sixth International Workshop on X-ray Radiation Damage to Biological Crystalline Samples
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      Research Papers

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