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      Interface Characteristics of Sapphire Direct Bonding for High-Temperature Applications

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          Abstract

          In this letter, we present a sapphire direct bonding method using plasma surface activation, hydrophilic pre-bonding, and high temperature annealing. Through the combination of sapphire inductively coupled plasma etching and the direct bonding process, a vacuum-sealed cavity employable for high temperature applications is achieved. Cross-sectional scanning electron microscopy (SEM) research of the bonding interface indicates that the two sapphire pieces are well bonded and the cavity structure stays intact. Moreover, the tensile testing shows that the bonding strength of the bonding interface is in excess of 7.2 MPa. The advantage of sapphire direct bonding is that it is free from the various problems caused by the mismatch in the coefficients of thermal expansion between different materials. Therefore, the bonded vacuum-sealed cavity can be potentially further developed into an all-sapphire pressure sensor for high temperature applications.

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          Most cited references15

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          Wafer-to-wafer bonding for microstructure formation

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            SEMICONDUCTOR WAFER BONDING

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              Fabrication of All-SiC Fiber-Optic Pressure Sensors for High-Temperature Applications

              Single-crystal silicon carbide (SiC)-based pressure sensors can be used in harsh environments, as they exhibit stable mechanical and electrical properties at elevated temperatures. A fiber-optic pressure sensor with an all-SiC sensor head was fabricated and is herein proposed. SiC sensor diaphragms were fabricated via an ultrasonic vibration mill-grinding (UVMG) method, which resulted in a small grinding force and low surface roughness. The sensor head was formed by hermetically bonding two layers of SiC using a nickel diffusion bonding method. The pressure sensor illustrated a good linearity in the range of 0.1–0.9 MPa, with a resolution of 0.27% F.S. (full scale) at room temperature.
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                Author and article information

                Journal
                Sensors (Basel)
                Sensors (Basel)
                sensors
                Sensors (Basel, Switzerland)
                MDPI
                1424-8220
                11 September 2017
                September 2017
                : 17
                : 9
                : 2080
                Affiliations
                [1 ]Science and Technology on Electronic Test & Measurement Laboratory, North University of China, Taiyuan 030051, China; 18434365707@ 123456163.com (W.L.); cyl029@ 123456126.com (Y.C.); pgjia@ 123456cqu.edu.cn (P.J.); xiongjijun@ 123456nuc.edu.cn (J.X.); hongyingping@ 123456nuc.edu.cn (Y.H.); leichengnuc@ 123456163.com (C.L.)
                [2 ]Key Laboratory of Instrumentation Science & Dynamic Measurement, Ministry of Education, North University of China, Taiyuan 030051, China
                [3 ]North Automatic Control Technology Institute, Taiyuan 030006, China; yaozong126@ 123456sina.com (Z.Y.); qilei19850224@ 123456163.com (L.Q.)
                Author notes
                [* ]Correspondence: liangtingnuc@ 123456nuc.edu.cn (T.L.); liuwenyi@ 123456nuc.edu.cn (W.L.); Tel.: +86-351-3920330 (T.L.); +86-351-3557385 (W.L.)
                Author information
                https://orcid.org/0000-0001-5883-2190
                Article
                sensors-17-02080
                10.3390/s17092080
                5621027
                28892010
                c1714fe5-2784-4c9d-b64d-a7910c4e7089
                © 2017 by the authors.

                Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license ( http://creativecommons.org/licenses/by/4.0/).

                History
                : 14 August 2017
                : 08 September 2017
                Categories
                Article

                Biomedical engineering
                sapphire,direct bonding,vacuum-sealed cavity,pressure sensor,high temperature

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