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      Methyl 3-(1 H-indole-3-carboxamido)propionate hemihydrate

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          Abstract

          The title compound, C 13H 14N 2O 3·0.5H 2O, was synthesized by the condensation of methyl 3-amino­propionate with 3-trichloro­acetyl­indole. The two organic mol­ecules in the asymmetric unit are both close to planar, with r.m.s. deviations from the best fit plane through all of the non-H atoms of 0.004 (2) Å for mol­ecule A and 0.006 (1) Å for mol­ecule B. Also, the five- and six-membered rings of the indole systems are inclined at 1.67 (8) and 1.50 (8)° in mol­ecules A and B, respectively. In the crystal structure, the organic molecules are connected by inter­molecular N—H⋯O hydrogen bonds, forming chains. O—H⋯O and N—H⋯O hydrogen-bond inter­actions involving the water molecules inter­link these chains, forming double chains approximately parallel to the a axis.

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          Author and article information

          Journal
          Acta Crystallogr Sect E Struct Rep Online
          Acta Cryst. E
          Acta Crystallographica Section E: Structure Reports Online
          International Union of Crystallography
          1600-5368
          01 June 2010
          26 May 2010
          26 May 2010
          : 66
          : Pt 6 ( publisher-idID: e100600 )
          : o1472
          Affiliations
          [a ]Department of Chemistry, Jinan University, Guangzhou, Guangdong 510632, People’s Republic of China
          Author notes
          Correspondence e-mail: xczeng@ 123456126.com
          Article
          sj2794 ACSEBH S1600536810018015
          10.1107/S1600536810018015
          2979597
          21579540
          eb75894d-a1d4-4111-84fe-c1da3deb64e3
          © Huang et al. 2010

          This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.

          History
          : 30 April 2010
          : 15 May 2010
          Categories
          Organic Papers

          Materials characterization
          Materials characterization

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