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      Correlation between flexural and indirect tensile strength of resin composite cements

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          Abstract

          Background

          To evaluate a potential correlation between flexural strength and indirect tensile strength in assessing the mechanical strength of resin composite cements.

          Methods

          Flexural strength ( n = 5) and indirect tensile strength ( n = 5) of 7 resin composite cements (RelyX Unicem 2 Automix [RXU], Panavia SA [PSA], Clearfil SA [CSA], Panavia F2.0 [PF2], Multilink Implant [MLI], DuoCem [DCM], Panavia 21 [P21]) were determined. Specimens were either auto-polymerized or dual-cured (except P21) and stored in water at 37 °C for 1 day prior to measurement. Flexural and indirect tensile strength of 4 cements (RXU, PSA, PF2, MLI) was additionally measured directly after curing and after 96 h water storage at 37 °C.

          Results

          Except for PF2, dual-cured specimens achieved higher flexural strength than auto-polymerized specimens. In the indirect tensile strength test differences in auto-polymerized and dual-cured specimens were only detected for RXU and DCM. A general non-linear correlation was found between flexural and indirect tensile strength values. However, strength values of auto-polymerized and dual-cured specimens did not generally correlate.

          Conclusions

          Flexural strength and indirect tensile strength of resin composite cements are correlated. At high strength values the indirect tensile test is less sensitive than the flexural test. The results suggest that the indirect tensile test may only be recommended as a screening test especially for low or medium strength resin composite cements.

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          Most cited references24

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          Mechanical and physical properties of contemporary dental luting agents.

          New luting agents, particularly with adhesive capability, are being introduced in an attempt to improve clinical success. Independent studies of basic comparative data are necessary to characterize these materials in relation to mechanical and physical properties. The purpose of this study was to compare the flexural strength, modulus of elasticity, and radiopacity and pH of representatives of 5 types (categories) of luting agents. The luting agents included a zinc phosphate, a conventional and a resin-modified glass ionomer, 2 dual-polymerizing resins ("photopolymerized" after mixing and "unphotopolymerized" conditions), and an auto-polymerizing resin. The specimens were prepared and the testing was conducted by 1 person to maximize standardization. Flexural strength (MPa) and modulus of elasticity (GPa) were determined on bar-shaped specimens (2 x 2 x 20 mm) at 24 hours and 3 months (n = 8). Radiopacity (mm Al) was measured by exposing 1 mm thick specimens along with an aluminum step wedge (n = 4). pH was measured using a pH electrode immediately after mixing; at 1, 5, 15, 30 minutes; and at 1, 2, 4, 6, and 24 hours (n = 4). The data were subjected to statistical analyses with analysis of variance and Duncan's multiple range test (P<.05). The resin luting agents (64 to 97 MPa) showed higher flexural strength than all other materials tested (7 to 27 MPa), with the "photopolymerized" (83 to 97 MPa) conditions higher than "unphotopolymerized" (64 to 81 MPa) (P<.0005). Zinc phosphate was the most radiopaque (6.4 mm Al) (P<.0001) and provided the highest rigidity (9.2 GPa) (P<.05). The autopolymerization resin cement was the most radiolucent (1.1 mm Al) (P<.0001). Zinc phosphate and conventional glass ionomer cements were the most acidic immediately after mixing (pH 1.5 to 2.2) but were the least acidic after 24 hours (pH 6.4 to 6.8) (P<.0001). Within the limitations of this study the data showed a wide variation of material properties. The dual-polymerization resin luting agents tested showed the best combination of mechanical and physical properties combined with the highest setting pH. Photopolymerization of these resin-based materials was necessary to maximize strength and rigidity.
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            Mechanical properties of resin cements with different activation modes.

            Dual-cured cements have been studied in terms of the hardness or degree of conversion achieved with different curing modes. However, little emphasis is given to the influence of the curing method on other mechanical properties. This study investigated the flexural strength, flexural modulus and hardness of four proprietary resin cements. Materials tested were: Enforce and Variolink II (light-, self- and dual-cured), RelyX ARC (self- and dual-cured) and C & B (self-cured). Specimens were fractured using a three-point bending test. Pre-failure loads corresponding to specific displacements of the cross-head were used for flexural modulus calculation. Knoop hardness (KHN) was measured on fragments obtained after the flexural test. Tests were performed after 24 h storage at 37 degrees C. RelyX ARC dual-cured showed higher flexural strength than the other groups. RelyX ARC and Variolink II depended upon photo-activation to achieve higher hardness values. Enforce showed similar hardness for dual- and self-curing modes. No correlation was found between flexural strength and hardness, indicating that other factors besides the degree of cure (e.g. filler content and monomer type) affect the flexural strength of composites. No statistical difference was detected in the flexural modulus among the different groups.
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              Morphological and bond strength evaluation of different resin cements to root dentin.

              This study correlated the morphological characteristics with the bond strengths of various resin cements used for bonding fiber posts to root canal dentin. Fifty glass-fiber posts (FRC Postec Plus) were luted into the root canals of extracted human anterior teeth using five resin cements (n = 10): Panavia F 2.0, PermaFlo DC, Variolink II, RelyX Unicem, and Clearfil Core. Before insertion of the post, the adhesive systems were labeled with fluorescein and the resin cement was labeled with rhodamine isothiocyanate. The roots were sectioned into three slices (of 2 mm thickness), and each slice was analyzed using confocal laser scanning microscopy in dual fluorescence mode to determine hybrid layer thickness, the number of resin tags, and the number of broken tags. Bond strengths were measured using a micro push-out test. Bond strengths to root canal dentin, as well as the morphological characteristics, were significantly affected by the materials. However, these factors did not correlate. The self-adhesive resin cement, which showed the formation of a hybrid layer and resin tags only sporadically, had the highest bond strengths. These results indicate that chemical interactions between the adhesive cement and hydroxyapatite may be more crucial for root dentin bonding than the ability of the same material to hybridize dentin.
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                Author and article information

                Contributors
                +41 61 267 26 37 , nadja.rohr@unibas.ch
                Journal
                Head Face Med
                Head Face Med
                Head & Face Medicine
                BioMed Central (London )
                1746-160X
                4 November 2016
                4 November 2016
                2016
                : 12
                : 29
                Affiliations
                Division of Dental Materials and Engineering, Clinic for Reconstructive Dentistry and Temporomandibular Disorders, University Hospital of Dental Medicine, University of Basel, Hebelstrasse 3, 4056 Basel, Switzerland
                Author information
                http://orcid.org/0000-0002-1218-4519
                Article
                128
                10.1186/s13005-016-0128-7
                5096060
                27809863
                fa44bb9f-f9a5-41de-a50b-33fd0c13eeda
                © The Author(s). 2016

                Open AccessThis article is distributed under the terms of the Creative Commons Attribution 4.0 International License ( http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution, and reproduction in any medium, provided you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made. The Creative Commons Public Domain Dedication waiver ( http://creativecommons.org/publicdomain/zero/1.0/) applies to the data made available in this article, unless otherwise stated.

                History
                : 23 June 2016
                : 26 October 2016
                Categories
                Research
                Custom metadata
                © The Author(s) 2016

                Orthopedics
                resin composite cement,curing mode,auto-polymerizing cement,dual-curing cement,flexural strength,indirect tensile strength,aging

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