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      Crystal structure of 4-(4-meth­oxy­phen­yl)-4′,4′-dimethyl-3- p-tolyl-3′,4′-di­hydro-1′ H,3 H-spiro­[isoxazole-5,2′-naphthalen]-1′-one

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          Abstract

          In the title compound, C 28H 27NO 3, the cyclo­hexa­none and isoxazole rings have envelope conformations, with the methyl­ene and spiro C atoms as the flaps, respectively. The mean plane of the isoxazole ring is inclined slightly to the p-tolyl ring, making a dihedral angle of 14.20 (9)°, and is nearly perpendicular to the mean plane through the tetra­lone moiety and to the meth­oxy­phenyl ring [dihedral angles = 83.41 (8) and 72.12 (9)°, respectively]. The crystal packing is stabilized mainly by van der Waals forces.

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          Author and article information

          Journal
          Acta Crystallogr E Crystallogr Commun
          Acta Crystallogr E Crystallogr Commun
          Acta Cryst. E
          Acta Crystallographica Section E: Crystallographic Communications
          International Union of Crystallography
          2056-9890
          01 December 2015
          21 November 2015
          21 November 2015
          : 71
          : Pt 12 ( publisher-idID: e151200 )
          : o981
          Affiliations
          [a ]Laboratoire de Chimie Organique, Faculté des Sciences Dhar el Mahraz, Université Sidi Mohammed Ben Abdellah, Fès, Morocco
          [b ]Laboratoire de Chimie du Solide Appliquée, Faculté des Sciences, Université Mohammed V de Rabat, Avenue Ibn Battouta, BP 1014, Rabat, Morocco
          Author notes
          Correspondence e-mail: alhouarig@ 123456gmail.com
          Article
          rz5177 ACSECI S2056989015022033
          10.1107/S2056989015022033
          4719934
          26870562
          06916253-811e-4b6b-bd02-bfbb1e6750e6
          © Akhazzane et al. 2015

          This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.

          History
          : 09 November 2015
          : 18 November 2015
          Categories
          Data Reports

          crystal structure,isoxazole,tetra­lone
          crystal structure, isoxazole, tetra­lone

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