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      In situ evidence for Paleoindian hematite quarrying at the Powars II site (48PL330), Wyoming

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          Significance

          Red ocher (also known as hematite) is relatively common in Paleoindian sites exceeding ca. 11,000 calibrated years B.P. in the Great Plains and Rocky Mountains of North America. Red ocher fulfilled a wide range of functions within Paleoindian societies, as indicated by its association with graves, caches, campsites, hide-working implements, and kill sites. To date, the Powars II site is the only red ocher quarry identified in the North American archaeological record north of Mesoamerica. Prior studies of Powars II were based on analyses of artifacts recovered from a redeposited context. This study presents in situ evidence for red ocher quarrying at Powars II.

          Abstract

          We present results from controlled excavations at the Powars II Paleoindian hematite quarry (48PL330), located in the foothills of the southern Rocky Mountains in Wyoming. We document a deeply buried, bedrock-adjacent stratum containing in situ evidence for hematite quarrying beginning ca. 12,840 to 12,505 calibrated years (cal) B.P. associated with the Clovis and Plainview cultural complexes. Later occupation by the Hell Gap cultural complex intruded within previous quarry tailings and likely dates to ca. 11,600 cal B.P. The earliest Clovis and Plainview occupations contain a diverse assemblage of stone and faunal artifacts indicative of hematite quarrying, weaponry production and repair, and other tasks, while the later Hell Gap occupation is primarily focused on hematite quarrying and the placement of items in piles within an abandoned quarry feature. In situ archaeological deposits at Powars II are distinguished from overlying ex situ strata by sediment characteristics, bone preservation, patina development on chipped stone artifacts, diagnostic weaponry assemblages, and damage to flake margins. Nonlocal chipped stone raw materials indicate ties to much of the North American Great Plains, suggesting that Powars II hematite may be found in sites throughout the American midcontinent.

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          Bone Collagen Quality Indicators for Palaeodietary and Radiocarbon Measurements

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            Towards High-Precision AMS: Progress and Limitations

            Precision and accuracy in accelerator mass spectrometry (AMS) dating relies on the systematic reduction of errors at all stages of the dating process, from sampling to AMS measurement. With new AMS systems providing much better precision and accuracy for the final stage of the process, we need to review the process as a whole to test the accuracy of reported results. A new High Voltage Engineering Europa (HVEE) AMS system was accepted at Oxford in September 2002. Since then, the system has been in routine use for AMS dating and here we report on our experiences during the first year. The AMS system itself is known to be capable of making measurements on single targets to a precision of better than 0.2% for the14C/13C ratio and better than 0.1% for the13C/12C ratio. In routine operation, we measure known-age wood to a precision of just above 0.3%, including uncertainties in background and pretreatment. At these levels, the scatter in results is no higher than reported errors, suggesting that uncertainties of ±25 to ±3014C yr can be reliably reported on single target measurements. This provides a test of all parts of the process for a particular material in a particular state of preservation. More generally, sample pretreatment should remove as much contamination as feasible from the sample while adding as little laboratory contamination as possible. For more complex materials, such as bone, there is clearly more work needed to prove good reproducibility and insignificant offsets in all circumstances. Strategies for testing accuracy and precision on unknown material are discussed here, as well as the possibilities of one day reaching precisions equivalent to errors of <±2014C yr.
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              Chemical, enzymatic and spectroscopic characterization of “collagen” and other organic fractions from prehistoric bones

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                Author and article information

                Journal
                Proc Natl Acad Sci U S A
                Proc Natl Acad Sci U S A
                pnas
                pnas
                Proceedings of the National Academy of Sciences of the United States of America
                National Academy of Sciences
                0027-8424
                1091-6490
                12 May 2022
                17 May 2022
                12 November 2022
                : 119
                : 20
                : e2201005119
                Affiliations
                [1] aOffice of the Wyoming State Archaeologist, University of Wyoming , Laramie, WY 82071;
                [2] bOxford Radiocarbon Accelerator Unit, School of Archaeology, University of Oxford , Oxford OX1 3TG, United Kingdom;
                [3] cDepartment of Anthropology, University of Wyoming , Laramie, WY 82071;
                [4] ddepartmentSunrise Historic and Prehistoric Preservation Society , Hartville, WY 82215
                Author notes
                1To whom correspondence may be addressed. Email: Spencer.pelton@ 123456wyo.gov .

                Edited by Charles Stanish, University of South Florida, Tampa, FL; received January 19, 2022; accepted April 4, 2022

                Author contributions: S.R.P., G.Z., and G.C.F. designed research; S.R.P., A.C., S.A., C.M., and E.K. performed research; S.R.P., L.B.-V., and C.K. analyzed data; L.B.-V. performed radiocarbon analysis; A.C. performed lithic analysis; S.A. and C.M. performed sediment analysis; C.K. performed three-dimensional photogrammetry; E.K. conducted faunal analysis; G.Z. and G.C.F. provided senior guidance; and S.R.P. wrote the paper.

                2Deceased September 6, 2020.

                Author information
                https://orcid.org/0000-0001-7429-8741
                https://orcid.org/0000-0001-5501-5347
                https://orcid.org/0000-0002-3152-833X
                https://orcid.org/0000-0002-9460-5312
                https://orcid.org/0000-0001-5001-5786
                https://orcid.org/0000-0002-3035-0699
                Article
                202201005
                10.1073/pnas.2201005119
                9171918
                35549550
                02690768-db58-442d-992e-be0816f97ce9
                Copyright © 2022 the Author(s). Published by PNAS.

                This article is distributed under Creative Commons Attribution-NonCommercial-NoDerivatives License 4.0 (CC BY-NC-ND).

                History
                : 04 April 2022
                Page count
                Pages: 9
                Categories
                402
                Social Sciences
                Anthropology

                ocher,younger dryas,clovis,quarrying
                ocher, younger dryas, clovis, quarrying

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