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      Large Area Stress Distribution in Crystalline Materials Calculated from Lattice Deformation Identified by Electron Backscatter Diffraction

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          Abstract

          We report a method to obtain the stress of crystalline materials directly from lattice deformation by Hooke's law. The lattice deformation was calculated using the crystallographic orientations obtained from electron backscatter diffraction (EBSD) technology. The stress distribution over a large area was obtained efficiently and accurately using this method. Wurtzite structure gallium nitride (GaN) crystal was used as the example of a hexagonal crystal system. With this method, the stress distribution of a GaN crystal was obtained. Raman spectroscopy was used to verify the stress distribution. The cause of the stress distribution found in the GaN crystal was discussed from theoretical analysis and EBSD data. Other properties related to lattice deformation, such as piezoelectricity, can also be analyzed by this novel approach based on EBSD data.

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          Direct measurement of triaxial strain fields around ferroelectric domains using X-ray microdiffraction.

          Ferroelectric materials, such as BaTiO(3), have piezoelectric properties that make them attractive for microelectronic and sensing applications. It is well known that the application of mechanical stress or electric field can alter the domain structure in ferroelectrics. Indeed, the constitutive behaviour of a ferroelectric is largely governed by the formation, movement and interaction of its domains. Therefore, it is crucial that the micromechanics of domains and their effect on internal stresses in ferroelectrics be understood. Here we show that the emerging technique of scanning X-ray microdiffraction can be used to measure directly, for the first time, the local triaxial strain fields around 90 degrees domains in single-crystal BaTiO(3). Specifically, residual strain maps in a region surrounding an isolated, approximately 40 microm wide, 90 degrees domain were obtained with 3 microm resolution, revealing significant residual strains. This information is critical for accurate micromechanical modelling of domain behaviour in ferroelectrics.
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            Author and article information

            Journal
            Sci Rep
            Sci Rep
            Scientific Reports
            Nature Publishing Group
            2045-2322
            05 August 2014
            2014
            : 4
            : 5934
            Affiliations
            [1 ]State Key Lab of Crystal Materials, Shandong University , Jinan250100, P. R. China
            Author notes
            Article
            srep05934
            10.1038/srep05934
            4121609
            25091314
            bdaabf6a-2c30-44c1-98df-fbf75f26f301
            Copyright © 2014, Macmillan Publishers Limited. All rights reserved

            This work is licensed under a Creative Commons Attribution 4.0 International License. The images or other third party material in this article are included in the article's Creative Commons license, unless indicated otherwise in the credit line; if the material is not included under the Creative Commons license, users will need to obtain permission from the license holder in order to reproduce the material. To view a copy of this license, visit http://creativecommons.org/licenses/by/4.0/

            History
            : 10 April 2014
            : 14 July 2014
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