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      The Mechanism of Water Oxidation: From Electrolysis via Homogeneous to Biological Catalysis

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          Investigation of the oxygen evolution reaction on Ti/IrO2 electrodes using isotope labelling and on-line mass spectrometry

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            X-ray absorption spectroscopy measurements of liquid water.

            Recent studies, based on X-ray absorption spectroscopy (XAS) and X-ray Raman scattering (XRS), have shown that the hydrogen bond network in liquid water consists mainly of water molecules with only two strong hydrogen bonds. Since this result is controversial, it is important to demonstrate the reliability of the experimental data, which is the purpose of this paper. Here we compare X-ray absorption spectra of liquid water recorded with five very different techniques sensitive to the local environment of the absorbing molecule. Overall, the spectra obtained with photon detection show a very close similarity and even the observable minor differences can be understood. The comparison demonstrates that XAS and XRS can indeed be applied reliably to study the local bonding of the water molecule and thus to reveal the hydrogen bond situation in bulk water.
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              Water Oxidation: A Robust All-Inorganic Catalyst

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                Author and article information

                Journal
                ChemCatChem
                ChemCatChem
                Wiley-Blackwell
                18673880
                18673899
                July 12 2010
                June 28 2010
                : 2
                : 7
                : 724-761
                Article
                10.1002/cctc.201000126
                fb6b4b24-b402-4730-b255-27277e60208b
                © 2010

                http://doi.wiley.com/10.1002/tdm_license_1.1

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