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      1-Acetyl-4-phenyl-5a,6,7,8,9,9a-hexa­hydro-5 H-1,5-benzodiazepin-2(1 H)-one

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          Abstract

          The seven-membered ring of the title compound, C 17H 20N 2O 2, adopts an approximate boat conformation while the cyclo­hexyl ring adopts a chair conformation. In the crystal, adjacent mol­ecules are linked by N—H⋯O hydrogen bonds into a zigzag chain running along the c axis of the monoclinic unit cell.

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          Author and article information

          Journal
          Journal ID (nlm-ta): Acta Crystallogr Sect E Struct Rep Online
          Journal ID (publisher-id): Acta Cryst. E
          Title: Acta Crystallographica Section E: Structure Reports Online
          Publisher: International Union of Crystallography
          ISSN (Electronic): 1600-5368
          Publication date Collection: 01 November 2009
          Publication date (Electronic): 07 October 2009
          Publication date PMC-release: 07 October 2009
          Volume: 65
          Issue: Pt 11 ( publisher-idID: e091100 )
          Page: o2657
          Affiliations
          [a ]Laboratoire de Chimie Organique Hétérocyclique, Pôle de Compétences Pharmacochimie, Université Mohammed V-Agdal, BP 1014 Avenue Ibn Batout, Rabat, Morocco
          [b ]Service Commun Rayons X, Université Paul Sabatier, Bâtiment 2R1, 118 route de Narbonne, 31062 Toulouse, France
          [c ]Hétérochimie Fondamentale et Appliquée, Université Paul Sabatier, UMR 5069, 118 Route de Narbonne, 31062 Toulouse, France
          [d ]Department of Chemistry, University of Malaya, 50603 Kuala Lumpur, Malaysia
          Author notes
          Correspondence e-mail: seikweng@ 123456um.edu.my
          Article
          Publisher ID: tk2546 Coden ID: ACSEBH Publisher Item ID: S1600536809039932
          DOI: 10.1107/S1600536809039932
          PMC ID: 2971313
          PubMed ID: 21578269
          SO-VID: 2f597143-d19b-4b46-97ed-346f29ce2229
          Copyright © © Benzeid et al. 2009
          License:

          This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.

          History
          Date received : 29 September 2009
          Date accepted : 01 October 2009
          Categories
          Subject: Organic Papers

          ScienceOpen disciplines: Materials characterization
          Data availability:
          ScienceOpen disciplines: Materials characterization

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