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      Dislocation substructures in pure aluminium after creep deformation as studied by electron backscatter diffraction

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          Abstract

          In the present work, electron backscatter diffraction is used to investigate the influence of crystal orientation and stress level on the dislocation structures generated during primary and steady-state creep in pure aluminium (99.8%). The goal is to characterize features of the microstructure with a statistically sound approach.

          Abstract

          In the present work, electron backscatter diffraction was used to determine the microscopic dislocation structures generated during creep (with tests interrupted at the steady state) in pure 99.8% aluminium. This material was investigated at two different stress levels, corresponding to the power-law and power-law breakdown regimes. The results show that the formation of subgrain cellular structures occurs independently of the crystallographic orientation. However, the density of these cellular structures strongly depends on the grain crystallographic orientation with respect to the tensile axis direction, with 〈111〉 grains exhibiting the highest densities at both stress levels. It is proposed that this behaviour is due to the influence of intergranular stresses, which is different in 〈111〉 and 〈001〉 grains.

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          Author and article information

          Contributors
          Role: Editor
          Journal
          J Appl Crystallogr
          J Appl Crystallogr
          J. Appl. Cryst.
          Journal of Applied Crystallography
          International Union of Crystallography
          0021-8898
          1600-5767
          01 August 2022
          05 July 2022
          05 July 2022
          : 55
          : Pt 4 ( publisher-idID: j220400 )
          : 860-869
          Affiliations
          [a ] Bundesanstalt für Materialforschung und -prüfung (BAM) , Unter Den Eichen 87, Berlin, 12205, Germany
          [b ]Department of Physical Metallurgy, Centro Nacional de Investigaciones Metalúrgicas (CENIM) , Avenida de Gregorio del Amo No. 8, Madrid, E-28040, Spain
          [c ]Institute of Physics and Astronomy, University of Potsdam , Karl-Liebknecht-Strasse 24–25, Potsdam, 14476, Germany
          SLAC National Accelerator Laboratory, Menlo Park, USA
          Author notes
          Author information
          https://orcid.org/0000-0002-5585-6637
          https://orcid.org/0000-0002-4330-7585
          https://orcid.org/0000-0001-6338-4062
          https://orcid.org/0000-0001-9632-3960
          Article
          te5088 JACGAR S1600576722005209
          10.1107/S1600576722005209
          9348881
          c5592a78-366f-4648-b9d2-446e8181e949
          © Itziar Serrano-Munoz et al. 2022

          This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.

          History
          : 17 December 2021
          : 13 May 2022
          Page count
          Pages: 10
          Funding
          Funded by: Ministerio de Economía y Competitividad
          This project was partially financed by the Spanish MINECO program, corresponding to Project MAT2017-83825-C4-1-R, and by the project Y2018/NMT-4668 Micro-Stress-MAP-C from Comunidad Autónoma de Madrid, Spain.
          Categories
          Research Papers

          Analytical chemistry
          creep,pure aluminium,electron backscatter diffraction (ebsd),cellular structures,power law and power-law breakdown

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