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      The effect of composite resin preheating on marginal adaptation of class II restorations

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          Abstract

          Background

          One of the problems with a high filler content composite resins is gap formation at restorative material–tooth interface. The present study investigated the effect of preheating composite resins on the formation of marginal gap in Cl II restorations.

          Material and Methods

          In this in vitro study Sixty Cl II cavities were prepared on the mesial and distal surfaces of 30 extracted premolar teeth. The gingival floor of cavities was placed 1 m below the CEJ. The samples were randomly allocated to 4 groups for restoration placement: group 1, Filtek P60 composite resin at room temperature; group 2, Filtek P60 composite resin at 68°C; group 3, X-tra fil composite resin at room temperature; and group 4, X-tra fil composite resin at 68°C. After a thermocycling procedure, the teeth were sectioned longitudinally in a buccolingual direction. Then the marginal gaps of the samples were measured at proximal and gingival margins under a scanning electron microscope at ×2000 magnification in µm. The data were analyzed with SPSS 21, using one-way ANOVA, post hoc Tukey tests and paired t-test (α=0.05).

          Results

          Groups 2 and 4 exhibited significantly lower marginal gaps, compared to groups 1 and 3, at both enamel ( P<0.0001 and P=0.001, respectively) and dentinal walls ( P<0.0001). In all the groups, there was significantly less marginal gaps at composite-enamel wall compared to composite-dentin wall interfaces ( P<0.0001). There was no significant difference between groups 1 and 3 and groups 2 and 4 in enamel walls ( p= 0.96, p= 0.99 respectively) and dentinal walls ( p= 0.85, p=0.98 respectively).

          Conclusions

          Preheating resulted in a decrease in marginal gaps in both composite resins. The effect of composite resin type on marginal adaptation was the same.

          Key words:Composite resin, dental marginal adaptation, preheating.

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          Most cited references27

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          Monomer conversion of pre-heated composite.

          The potential for maximizing conversion of room-temperature, photoactivated resin composite in the oral environment is limited. Pre-heating composite prior to light-curing is hypothesized to increase monomer conversion and reduce the duration of light exposure. Composite temperature was controlled at between 3 degrees C and 60 degrees C prior to exposure with a conventional quartz-tungsten-halogen curing unit: 5, 10, 20, or 40 sec. Monomer conversion was calculated from infrared spectra at 0 mm (top) and 2-mm-deep surfaces 5 min after light initiation. A strong, positive correlation existed between temperature and monomer conversion: top r(2) = 0.999, 2 mm r(2) = 0.998. Conversion ranged from 31.6% (3 degrees C) to 67.3% (60 degrees C). The duration of light exposure, reduced by 50 to 75% with pre-heated composite, yielded the same or significantly higher conversion (p = 0.001) than with control (22 degrees C, 20 sec). Both hypotheses were accepted: Pre-heating composite prior to photoactivation provides greater conversion requiring reduced light exposure than with room-temperature composite.
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            Composite pre-heating: effects on marginal adaptation, degree of conversion and mechanical properties.

            This study evaluated the effect of composite pre-polymerization temperature and energy density on the marginal adaptation (MA), degree of conversion (DC), flexural strength (FS), and polymer cross-linking (PCL) of a resin composite (Filtek Z350, 3M/ESPE). For MA, class V cavities (4 mm x 2 mm x 2 mm) were prepared in 40 bovine incisors. The adhesive system Adper Single Bond 2 (3M/ESPE) was applied. Before being placed in the cavities, the resin composite was either kept at room-temperature (25 degrees C) or previously pre-heated to 68 degrees C in the Calset device (AdDent Inc., Danbury, CT, USA). The composite was then light polymerized for 20 or 40s at 600 mW/cm(2) (12 or 24 J/cm(2), respectively). The percentage of gaps was analyzed by scanning electron microscopy, after sectioning the restorations and preparing epoxy resin replicas. DC (n=3) was obtained by FT-Raman spectroscopy on irradiated and non-irradiated composite surfaces. FS (n=10) was measured by the three-point-bending test. KHN (n=6) was measured after 24 h dry storage and again after immersion in 100% ethanol solution for 24h, to calculate PCL density. Data were analyzed by appropriate statistical analyses. The pre-heated composite showed better MA than the room-temperature groups. A higher number of gaps were observed in the room-temperature groups, irrespective of the energy density, mainly in the axial wall (p 0.05). Pre-heating the composite prior to light polymerization similar in a clinical situation did not alter the mechanical properties and monomer conversion of the composite, but provided enhanced composite adaptation to cavity walls. Copyright 2010 Academy of Dental Materials. Published by Elsevier Ltd. All rights reserved.
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              The effects of light intensity, temperature, and comonomer composition on the polymerization behavior of dimethacrylate dental resins.

              One of the most common combinations for the organic phase of dental restorative materials is BisGMA (2,2bis[4-(2-hydroxy-3-methacryloyloxypropoxy) phenyl]propane) and TEGDMA (triethylene glycol dimethacrylate). However, this copolymer has some drawbacks, such as volume shrinkage during cure and lack of complete double-bond conversion. If the properties of this system are to be improved, an attempt must be made to understand the underlying kinetics of the reaction. This work examines the effects of light intensity, temperature, and composition on the polymerization behavior of BisGMA/TEGDMA copolymerizations. Using differential scanning calorimetry, we monitored the rates of photopolymerization for various experimental conditions. The BisGMA/TEGDMA copolymerization behaved similarly to other dimethacrylate systems and exhibited diffusion-controlled kinetics. It was found that the maximum rate of polymerization was significantly affected by the intensity of the light, and the temperature of the polymerization affected the conversion at which the maximum rate occurred. When the composition of the mixture was varied, it was discovered that the viscosity of the system played a significant role in the polymerization rate and the onset of reaction-diffusion-controlled termination. Mixtures which contained from 50 wt% to 75 wt% BisGMA displayed the highest maximum rate. This feature suggests that TEGDMA is an excellent diluent, since it increases the mobility of the reacting medium; however, the high reactivity is due to the presence of BisGMA. Therefore, based on compositional dependence, we conclude that the BisGMA portion of the mixture largely controls the polymerization mechanisms and kinetics.
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                Author and article information

                Journal
                J Clin Exp Dent
                J Clin Exp Dent
                Medicina Oral S.L.
                Journal of Clinical and Experimental Dentistry
                Medicina Oral S.L.
                1989-5488
                1 July 2020
                July 2020
                : 12
                : 7
                : e682-e687
                Affiliations
                [1 ]Associate professor, Department of Operative Dentistry, School of Dentistry, Guilan University of Medical Sciences, Rasht, Iran
                [2 ]Assistant professor, Department of Operative Dentistry, School of Dentistry, Guilan University of Medical Sciences, Rasht, Iran
                [3 ]Dentist, School of Dentistry, Guilan University of Medical Sciences, Rasht, Iran
                Author notes
                Guilan University of Medical Science School of dentistry, Lacan Road, Gas Square Rasht, Iran. Post Cod: 4194173774 , E-mail: minanasseralavi@ 123456yahoo.com
                Article
                56625
                10.4317/jced.56625
                7462384
                32905021
                ccd066c6-d509-48a3-97f6-c1786a6ded5d
                Copyright: © 2020 Medicina Oral S.L.

                This is an open-access article distributed under the terms of the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

                History
                : 8 January 2020
                : 3 December 2019
                Categories
                Research
                Operative Dentistry and Endodontics

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